Excerpt from Preparation of New Methylenedioxyphenyl Compounds and Acylbenzals
Treatment of the toluenethiol with sodium.ethylate and ethylene chlorohydrin (windus and Shildneckn) gave 2-chloropiperonyl)thioethanol (ii, R Cl; R' chqsczhloh) in 73 percent or its bromo analog i... n 52 percent yield. The thioether-alcohols obtained were reacted with thionyl chloride (kirner and'windus Ig) and the half-mustard gas molecules (ii, R Cl or Br; R' chqsczhlcl) were produced in 67 and 74 percent yields, respectively.
The vesicant properties of these compounds, if any, were not ascertained.
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